Journal Description
Journal of Composites Science
Journal of Composites Science
is an international, peer-reviewed, open access journal on the science and technology of composites published monthly online by MDPI.
- Open Access— free for readers, with article processing charges (APC) paid by authors or their institutions.
- High Visibility: indexed within Scopus, ESCI (Web of Science), Inspec, CAPlus / SciFinder, and other databases.
- Journal Rank: JCR - Q2 (Materials Science, Composites) / CiteScore - Q1 (Engineering (miscellaneous))
- Rapid Publication: manuscripts are peer-reviewed and a first decision is provided to authors approximately 18.5 days after submission; acceptance to publication is undertaken in 3.7 days (median values for papers published in this journal in the first half of 2024).
- Recognition of Reviewers: reviewers who provide timely, thorough peer-review reports receive vouchers entitling them to a discount on the APC of their next publication in any MDPI journal, in appreciation of the work done.
Impact Factor:
3.0 (2023);
5-Year Impact Factor:
3.3 (2023)
Latest Articles
Investigation of the Effect of Preparation Parameters on the Structural and Mechanical Properties of Gelatin/Elastin/Sodium Hyaluronate Scaffolds Fabricated by the Combined Foaming and Freeze-Drying Techniques
J. Compos. Sci. 2024, 8(10), 408; https://doi.org/10.3390/jcs8100408 - 4 Oct 2024
Abstract
This paper aimed to evaluate the effects of different preparation parameters, including agitation speed, agitation time, and chilling temperature, on the structural and mechanical properties of a novel gelatin/elastin/sodium hyaluronate tissue engineering scaffold, recently developed by our research group. Fabricated using a combination
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This paper aimed to evaluate the effects of different preparation parameters, including agitation speed, agitation time, and chilling temperature, on the structural and mechanical properties of a novel gelatin/elastin/sodium hyaluronate tissue engineering scaffold, recently developed by our research group. Fabricated using a combination of foaming and freeze-drying techniques, the scaffolds were assessed to understand how these parameters influence their morphology, internal microstructure, porosity, mechanical properties, and degradation behavior. The fabrication process used in this study involved preparing a homogeneous aqueous solution containing 8% gelatin, 2% elastin, and 0.5% sodium hyaluronate (w/v), which was then subjected to mechanical agitation at speeds of 500, 1000, and 1500 rpm for durations of 5, 15, and 25 min. This mixture was subsequently frozen at −20 °C and −80 °C, followed by freeze-drying and cross-linking. Morphological analyses using laser microscopy and scanning electron microscopy (SEM) demonstrated that the scaffolds had pore sizes ranging from 100 to 300 µm, which are conducive to effective cell interaction and tissue regeneration. This confirmed the efficacy of the combined foaming and freeze-drying method in creating highly interconnected porous structures. Our findings indicated that chilling temperature slightly influenced pore size. In contrast, higher agitation speeds and longer duration times led to increased porosity and degradation rate but decreased modulus. Mathematical estimators were developed for the porosity and compressive modulus of the scaffolds by statistical analysis of the preparation parameters. The estimators were validated experimentally, with the error between estimated and experimental values being less than 6% for porosity and less than 21% for compressive modulus.
Full article
(This article belongs to the Special Issue Advanced Composite Materials from Natural and Synthetic Sources: Fabrication, Characterization and Practical Application, Volume II)
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Open AccessArticle
Bond Strength and Corrosion Protection Properties of Hot-Dip Galvanized Prestressing Reinforcement in Normal-Strength Concrete
by
Petr Pokorný, Tomáš Chobotský, Nikola Prodanovic, Veronika Steinerová and Karel Hurtig
J. Compos. Sci. 2024, 8(10), 407; https://doi.org/10.3390/jcs8100407 - 4 Oct 2024
Abstract
Several prestressing reinforced structures have recently collapsed due to chloride-induced steel corrosion. This study investigates the effect of the corrosion of hot-dip galvanized conventional prestressing steel reinforcement under hydrogen evolution on bond strength in normal-strength concrete. The impact of hydrogen evolution on the
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Several prestressing reinforced structures have recently collapsed due to chloride-induced steel corrosion. This study investigates the effect of the corrosion of hot-dip galvanized conventional prestressing steel reinforcement under hydrogen evolution on bond strength in normal-strength concrete. The impact of hydrogen evolution on the porosity of cement paste at the interfacial transition zone (ITZ) is verified through image analysis. The whole surface of prestressing strands is hot-dip galvanized, and their corrosion behavior when embedded in the cement paste is investigated by measuring the time dependence of the open-circuit potential. Concerning the uniformity of the hot-dip galvanized coating and its composition, it is advisable to coat the individual wires of the prestressing reinforcement and subsequently form a strand. It is demonstrated that the corrosion of the coating under the evolution of hydrogen in the cement paste reduces the bond strength of hot-dip galvanized reinforcement in normal-strength concrete. Image analysis after 28 days of cement paste aging indicates insignificant filling of hydrogen-generated pores by zinc corrosion products. Applying an additional surface treatment (topcoat) stable in an alkaline environment is necessary to avoid corrosion of the coating under hydrogen evolution and limit the risk of bond strength reduction.
Full article
(This article belongs to the Section Composites Manufacturing and Processing)
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Stress Analysis of Glass Fiber-Reinforced Polymer Lap Joints with Modified Adhesives at Various Temperatures
by
Hasan Caglar, Sridhar Idapalapati, Mohit Sharma and Chian Kerm Sin
J. Compos. Sci. 2024, 8(10), 406; https://doi.org/10.3390/jcs8100406 - 4 Oct 2024
Abstract
This study examines stress distributions in adhesive joints under various loading and temperature conditions. Finite element analysis (FEA) was employed to compute the peel and shear stresses at the adhesive interface and bondline mid-section. Dependency analysis shows that mid-section peel stress significantly impacts
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This study examines stress distributions in adhesive joints under various loading and temperature conditions. Finite element analysis (FEA) was employed to compute the peel and shear stresses at the adhesive interface and bondline mid-section. Dependency analysis shows that mid-section peel stress significantly impacts the experimental shear strength of SLJs more than shear stress. This insight highlights the need to carefully analyze peel stress and bending moment factors. The analytical solutions proposed by Goland and Reissner were analyzed with modifications by Hart-Smith and Zhao. Hart-Smith’s approach performed more effectively, especially when the adhesive layer thickness (ta) was 0.5 mm and the overlap length to thickness ratio (c/ta) was ≥20. FEA revealed stress distributions at the adhesive/adherend interface and bondline mid-section. DP490 adhesive joints exhibited lower stresses than EA9696. Temperature variations significantly affected joint behavior, particularly above the adhesive’s glass transition temperature (Tg). Both EA9696 and DP490 adhesive joints displayed distinct responses to stress and temperature changes. The parabolic and biquadratic solutions for functionally graded adhesive (FGA) joints were compared. The biquadratic solution consistently yielded higher shear and peel stress values, with an increase ranging from 15% to 71% compared to the parabolic solution at various temperatures because of the larger gradient of the Young’s modulus distribution near the overlap ends. The ratio of peak peel stress to peak shear stress suggests that selecting an adhesive with a superior peel strength or primarily reducing the peak peel stress by functionally grading is advisable, particularly if the adhesive is brittle. The comparison of stress distributions emphasizes the importance of selecting adhesives based on stress type, temperature, and solution methods in optimizing adhesive bonding applications. These findings provide valuable insights for thermomechanical applications where thermal stimuli may be used for controlled debonding.
Full article
(This article belongs to the Special Issue Polymer Composites and Fibers, 3rd Edition)
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Fire Safety and Impact and Frost Resistance of Basalt Fiber-Reinforced Polysiloxane Matrix Composite Processed under Partial Pyrolysis Conditions
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Martin Černý, Zdeněk Chlup, Ján Kužma, Milan Růžička, Libor Ševčík, Petr Kácha, Jana Schweigstillová, Jaroslava Svítilová and Adam Strachota
J. Compos. Sci. 2024, 8(10), 405; https://doi.org/10.3390/jcs8100405 - 3 Oct 2024
Abstract
The study focuses on developing a fiber-reinforced composite that would exhibit good mechanical properties and climate resistance, and fire safety parameters would surpass commonly used fiber-reinforced polymers. The subject of development is a polysiloxane thermoset matrix reinforced with basalt fibers, which is processed
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The study focuses on developing a fiber-reinforced composite that would exhibit good mechanical properties and climate resistance, and fire safety parameters would surpass commonly used fiber-reinforced polymers. The subject of development is a polysiloxane thermoset matrix reinforced with basalt fibers, which is processed by partial pyrolysis at 650 °C after curing. The heat release rate test showed virtually zero heat released, and the toxicity test showed only a very low amount of carbon monoxide. The flammability test showed no ignition, no radiation, and no glow. Composites for mechanical tests were prepared in three variants differing in the distribution of reinforcement. Due to the intended use of the composite for thin-walled panels or shells of buildings, the mechanical properties were compared in identical tests with fiber cement plates. The flexural strength of the composites was 3 to 10 times, and the impact energy was 10 to 100 times higher than the values measured on fiber cement, depending on the type and orientation of the composite. The flexural strength measured after 240 freeze–thaw conditioning cycles is higher than fiber cement by 1.3 to 2 times. The climate resistance of the composite should be the subject of further development.
Full article
(This article belongs to the Section Fiber Composites)
Open AccessArticle
Mechanical Analysis of Corrugated Cardboard Subjected to Shear Stresses
by
Florin Ionut Boaca, Sorin Cananau, Andrei Calin, Mihai Bucur, Delia Alexandra Prisecaru and Marilena Stoica
J. Compos. Sci. 2024, 8(10), 404; https://doi.org/10.3390/jcs8100404 - 3 Oct 2024
Abstract
Corrugated cardboard is widely used for packaging due to its sturdiness and lightweight properties. However, its ability to withstand lateral forces during handling, transportation, and storage is critical for maintaining its structural integrity. In this study, the problem of understanding and quantifying the
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Corrugated cardboard is widely used for packaging due to its sturdiness and lightweight properties. However, its ability to withstand lateral forces during handling, transportation, and storage is critical for maintaining its structural integrity. In this study, the problem of understanding and quantifying the strain experienced by corrugated cardboard boxes under shear stresses at various points in their lifecycle is addressed. Specifically, a precise methodology for testing shear stresses was developed and validated, enhancing the understanding of the material’s behaviour. Several key problems are addressed in this research, including the quantification of the amount of strain experienced by cardboard boxes from a warehouse to the final delivery, the development of a reliable testing methodology to measure shear stresses, and the understanding of the mechanical behaviour and structural integrity of corrugated cardboard under these conditions. It is anticipated that the findings will improve the design and durability of corrugated cardboard packaging, ensuring better performance during transportation and storage. This research contributes to the optimisation of logistics, the improvement of packaging quality, and the support of sustainable development by enhancing the reuse and recyclability of corrugated cardboard.
Full article
(This article belongs to the Topic Modern Material Technologies Intended for Industrial Applications)
Open AccessArticle
Processing Influence on the Properties of Injection-Molded Wood Plastic Composites
by
Christoph Burgstaller and Károly Renner
J. Compos. Sci. 2024, 8(10), 403; https://doi.org/10.3390/jcs8100403 - 3 Oct 2024
Abstract
Wood–plastic composites (WPCs) utilize wood particles as the reinforcing phase. These particles are susceptible to thermal degradation, which can happen while processing the WPCs in usual thermoplastic processes. In this work, we investigated the influence of different processing parameters in injection molding and
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Wood–plastic composites (WPCs) utilize wood particles as the reinforcing phase. These particles are susceptible to thermal degradation, which can happen while processing the WPCs in usual thermoplastic processes. In this work, we investigated the influence of different processing parameters in injection molding and their influence on WPC properties. To achieve that, WPCs with wood contents ranging from 10 to 50 wt% were processed using different process settings, and then characterized using mechanical testing and appearance changes. We found that the melt temperature showed a major influence, due to degrading the interface between the wood and the polymer matrix, while other parameters, like mold temperature and dwell pressure, showed only minor influence. Overall, the WPCs exhibited good process stability and, with proper process settings, their performance can be improved.
Full article
(This article belongs to the Special Issue Composites: A Sustainable Material Solution)
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Synthesis of a New Composite Material Derived from Cherry Stones and Sodium Alginate—Application to the Adsorption of Methylene Blue from Aqueous Solution: Process Parameter Optimization, Kinetic Study, Equilibrium Isotherms, and Reusability
by
Cristina-Gabriela Grigoraș and Andrei-Ionuț Simion
J. Compos. Sci. 2024, 8(10), 402; https://doi.org/10.3390/jcs8100402 - 3 Oct 2024
Abstract
Purifying polluted water is becoming a crucial concern to meet quantity and quality demands as well as to ensure the resource’s sustainability. In this study, a new material was prepared from cherry stone powder and sodium alginate, and its capacity to remove methylene
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Purifying polluted water is becoming a crucial concern to meet quantity and quality demands as well as to ensure the resource’s sustainability. In this study, a new material was prepared from cherry stone powder and sodium alginate, and its capacity to remove methylene blue (MB) from water was determined. The characterization of the resulting product, performed via scanning electron microscopy (SEM) and Fourier-transform infrared spectroscopy (FTIR), revealed that the raw material considered for the synthesis was successfully embedded in the polymeric matrix. The impact of three of the main working parameters (pH 3–9, adsorbent dose 50–150 g/L, contact time 60–180 min) on the retention of MB was evaluated through response surface methodology with a Box–Behnken design. In the optimal settings, a removal efficiency of 80.46% and a maximum sorption capacity of 0.3552 mg/g were recorded. MB retention followed the pseudo-second-order kinetic and was suitably described by Freundlich, Khan, Redlich–Peterson, and Sips isotherm models. The experimental results show that the synthesized composite can be used for at least three successive cycles of MB adsorption. From these findings, it can be concluded that the use of the cherry-stone-based adsorbent is environmentally friendly, and efficacious in the removal of contaminants from the water environment.
Full article
(This article belongs to the Special Issue Theoretical and Computational Investigation on Composite Materials)
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A Numerical Framework of Simulating Flow-Induced Deformation during Liquid Composite Moulding
by
Hatim Alotaibi, Constantinos Soutis, Dianyun Zhang and Masoud Jabbari
J. Compos. Sci. 2024, 8(10), 401; https://doi.org/10.3390/jcs8100401 - 3 Oct 2024
Abstract
Fibre deformation (or shearing of yarns) can develop during the liquid moulding of composites due to injection pressures or polymerisation (cross-linking) reactions (e.g., chemical shrinkage). On that premise, this may also induce potential residual stress–strain, warpage, and design defects in the composite part.
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Fibre deformation (or shearing of yarns) can develop during the liquid moulding of composites due to injection pressures or polymerisation (cross-linking) reactions (e.g., chemical shrinkage). On that premise, this may also induce potential residual stress–strain, warpage, and design defects in the composite part. In this paper, a developed numerical framework is customised to analyse deformations and the residual stress–strain of fibre (at a micro-scale) and yarns (at a meso-scale) during a liquid composite moulding (LCM) process cycle (fill and cure stages). This is achieved by linking flow simulations (coupled filling–curing simulation) to a transient structural model using ANSYS software. This work develops advanced User-Defined Functions (UDFs) and User-Defined Scalers (UDSs) to enhance the commercial CFD code with extra models for chemorheology, cure kinetics, heat generation, and permeability. Such models will be hooked within the conservation equations in the thermo-chemo-flow model and hence reflected by the structural model. In doing so, the knowledge of permeability, polymerisation, rheology, and mechanical response can be digitally obtained for more coherent and optimised manufacturing processes of advanced composites.
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(This article belongs to the Special Issue Liquid Processing for Manufacturing of Composite Materials: Experimental Techniques and Numerical Modelling)
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Tuning of Particle Size of Zeolitic Imidazolate Framework-7 via Rapid Synthesis Duration for CH4 Adsorption
by
Li-Xing (Joey) Chai, Alia Syuhada Abd Rahman and Yin Fong Yeong
J. Compos. Sci. 2024, 8(10), 400; https://doi.org/10.3390/jcs8100400 - 2 Oct 2024
Abstract
In this work, zeolite imidazolate framework-7 (ZIF-7) nanoparticles are synthesized via a solvothermal method and rapid synthesis durations of 1 h and 3 h. The effect of the synthesis duration on the structural properties of ZIF-7 was characterized by XRD and FESEM analyses.
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In this work, zeolite imidazolate framework-7 (ZIF-7) nanoparticles are synthesized via a solvothermal method and rapid synthesis durations of 1 h and 3 h. The effect of the synthesis duration on the structural properties of ZIF-7 was characterized by XRD and FESEM analyses. Subsequently, CH4 single gas adsorption over ZIF-7 nanoparticles was examined using the volumetric method at room temperature and pressure ranging from 2 to 9 bar. The results showed that the synthesized ZIF-7 adsorbents were highly crystalline with a well-defined and homogeneous particle size distribution of 50–60 nm. It was found that increasing the synthesis duration from 1 h to 3 h did not amend the structure and morphology of the resultant samples significantly, mainly due to the short synthesis duration. Meanwhile, the CH4 adsorbed by ZIF-7 nanoparticles increased with rising pressure for both samples, and the ZIF-7 nanoparticles synthesized at 3 h showed a greater adsorption capacity than that of 1 h, mainly due to its higher crystallinity and well-developed pore structure. The ZIF-7 synthesized at 3 h demonstrated an adsorption capacity up to 2.2 mol/kg, which was higher than those values reported in the literature for micron-sized ZIF-7 samples. The CH4 gas adsorption behavior of ZIF-7 nanoparticles synthesized at 1 h and 3 h were well predicted by the Langmuir isotherm model, with coefficients of determination, R2, of 0.9994 and 0.9982, respectively.
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(This article belongs to the Section Nanocomposites)
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Extrusion and Injection Molding of Polyethylene Loaded with Recycled Textiles: Mechanical Performance and Thermal Conductivity
by
Mateo Gasselin, Adib Kalantar, Sofi Karlsson, Peter Leisner, Mikael Skrifvars and Pooria Khalili
J. Compos. Sci. 2024, 8(10), 399; https://doi.org/10.3390/jcs8100399 - 2 Oct 2024
Abstract
The aim of this project was to assess the thermal conductivity of polyethylene (PE) filled with carbon black (CB), specifically for geothermal pipes. The project explored the potential modification of PE’s thermal conductivity by incorporating recycled textile fibers. Different types of shredded recycled
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The aim of this project was to assess the thermal conductivity of polyethylene (PE) filled with carbon black (CB), specifically for geothermal pipes. The project explored the potential modification of PE’s thermal conductivity by incorporating recycled textile fibers. Different types of shredded recycled fibers were tested, including two types of polyamide fibers with varying contaminations and one type of polyester fiber. Following several preparation steps, various composite materials were manufactured and compared to bulk PE using various testing methods: Differential Scanning Calorimetry analysis (DSC), mechanical testing (flexural and tensile), and laser flash analysis (LFA). The results revealed alterations in the mechanical properties of the composite materials in comparison to PE filled with CB. The LFA tests demonstrated the effectiveness in reducing polymer thermal diffusivity at higher temperatures, particularly when the material was loaded with recycled polyester fillers.
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(This article belongs to the Special Issue Composites: A Sustainable Material Solution)
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Investigation of Tribological Behavior of PTFE Composites Reinforced with Bronze Particles by Taguchi Method
by
Ferit Ficici, Ismail Ozdemir, Thomas Grund and Thomas Lampke
J. Compos. Sci. 2024, 8(10), 398; https://doi.org/10.3390/jcs8100398 - 2 Oct 2024
Abstract
Reinforced PTFE materials can be designed to show high mechanical stability against harder materials under sliding wear conditions. Especially bearing metal-reinforced PTFE is of high practical interest. In this class of materials, bronze-filled PTFE was reported to obtain high wear resistance, a low
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Reinforced PTFE materials can be designed to show high mechanical stability against harder materials under sliding wear conditions. Especially bearing metal-reinforced PTFE is of high practical interest. In this class of materials, bronze-filled PTFE was reported to obtain high wear resistance, a low coefficient of friction (COF), and excellent self-lubrication properties in sliding conditions. In the statistical approach of this work, PTFE composites reinforced with 25 vol%, 40 vol%, and 60 vol% bronze particles were evaluated against pure PTFE regarding wear behavior under varied wear test parameters, i.e., material, normal load, and sliding speed. Wear tests were planned to use a standard orthogonal array based on the Taguchi design method. An analysis of variance test was utilized to quantify the effects of test parameters on the wear behavior of the bronze/PTFE composites and pure PTFE. According to the variance analysis, the material type has the largest influence on the COF and the specific wear rate (SWR) under test conditions of this work. Both COF and SWR were found to be influenced by the material type (29.83% and 96.16%), the normal load (33.34% and 0.95%), and sliding speed (9.14% and 1.28%). The lowest SWR and COF values were achieved at the optimum wear test conditions where the wear test parameters were 1 m/s sliding speed (A4B2C2) at PTFE + 60 vol.% bronze reinforced composite 50 N application load and 0.32 m/s sliding speed (A4B3C1) at PTFE + 60 vol.% bronze reinforced composite 100 N application load, respectively.
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(This article belongs to the Section Polymer Composites)
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Nitrogen-Doped Borophene Quantum Dots: A Novel Sensing Material for the Detection of Hazardous Environmental Gases
by
Kriengkri Timsorn and Chatchawal Wongchoosuk
J. Compos. Sci. 2024, 8(10), 397; https://doi.org/10.3390/jcs8100397 - 1 Oct 2024
Abstract
Toxic gases emitted by industries and vehicles cause environmental pollution and pose significant health risks which are becoming increasingly dangerous. Therefore, the detection of the toxic gases is crucial. The development of gas sensors with high sensitivity and fast response based on nanomaterials
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Toxic gases emitted by industries and vehicles cause environmental pollution and pose significant health risks which are becoming increasingly dangerous. Therefore, the detection of the toxic gases is crucial. The development of gas sensors with high sensitivity and fast response based on nanomaterials has garnered significant interest. In this work, we studied the adsorption behavior of wheel structures of pristine and nitrogen functionalized borophene quantum dots for major hazardous environmental gases, such as NO2, CO2, CO, and NH3. The self-consistent-charge density-functional tight-binding method (SCC-DFTB) method was performed to investigate structural geometries, the most favorable adsorption sites, charge transfer, total densities of states, and electronic properties of the structures before and after adsorption of the gas molecules. Based on calculated results, it was found that the interaction between the borophene quantum dots and the gas molecules was chemisorption. The functionalized nitrogen atom contributed to impurity states, leading to higher adsorption energies of the functionalized borophene quantum dots compared to the pristine ones. Total densities of states revealed insights into electronic properties of gas molecules adsorbed on borophene quantum dots. The nitrogen-doped borophene quantum dots demonstrated excellent performance as a sensing material for hazardous environmental gases, especially CO2.
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(This article belongs to the Special Issue Theoretical and Computational Investigation on Composite Materials)
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Characterisation of the Mechanical Properties of Natural Fibre Polypropylene Composites Manufactured with Automated Tape Placement
by
Alexander Legenstein, Lukas Haiden, Michael Feuchter and Ewald Fauster
J. Compos. Sci. 2024, 8(10), 396; https://doi.org/10.3390/jcs8100396 - 1 Oct 2024
Abstract
The integration of natural fibre thermoplastic composites, particularly those combining flax fibres with polypropylene, offers a promising alternative to traditional synthetic composites, emphasising sustainability in composite materials. This study investigates the mechanical properties of flax/polypropylene composites manufactured using flashlamp automated tape placement and
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The integration of natural fibre thermoplastic composites, particularly those combining flax fibres with polypropylene, offers a promising alternative to traditional synthetic composites, emphasising sustainability in composite materials. This study investigates the mechanical properties of flax/polypropylene composites manufactured using flashlamp automated tape placement and press consolidation, individually and in combination. Tensile, compression, three-point bending, and double cantilever beam tests are utilised for comparing these manufacturing processes and the mechanical performance of the resulting composites. The microstructure of the tapes is investigated using cross-sectional microscopy, and the thermophysical behaviour is analysed utilising thermogravimetric analysis and differential scanning calorimetry. The temperature during placement is monitored using an infrared camera, and the pressure is mapped with pressure-sensitive films. The natural fibre tapes show a good aptitude for being manufactured with automated tape placement. The tensile performance of tapes manufactured with automated tape placement is close to that of press consolidated samples. Compression, flexural properties, and the mode I fracture toughness critical energy release rate all benefit from a second consolidation step.
Full article
(This article belongs to the Special Issue Advances in Continuous Fiber Reinforced Thermoplastic Composites)
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Fracture Mechanisms and Toughness in Polymer Nanocomposites: A Brief Review
by
Theodor Stern and Gad Marom
J. Compos. Sci. 2024, 8(10), 395; https://doi.org/10.3390/jcs8100395 - 1 Oct 2024
Abstract
This article underlines the observation that, unlike the underperformance of nanocomposites in as far as their static mechanical properties of modulus and strength are concerned, fracture toughness exhibits exceptional behavior. This is attributed to the fact that fracture toughness expresses a measure of
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This article underlines the observation that, unlike the underperformance of nanocomposites in as far as their static mechanical properties of modulus and strength are concerned, fracture toughness exhibits exceptional behavior. This is attributed to the fact that fracture toughness expresses a measure of the energy absorbed in crack propagation, namely, the energy involved in creating new surface area, which, in turn, is controlled by a specific type of energy-dissipating interaction of the crack front with nanoparticles. This concise review focuses on two micromechanisms that are considered representative of energy dissipation due to their frequent presence in nanocomposites of both nanoparticles and nanofibers. Examples taken from recent relevant articles are presented to showcase fracture toughness improvements by nanoparticles.
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(This article belongs to the Special Issue Characterization of Polymer Nanocomposites)
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Open AccessArticle
Recycled Low Density Polyethylene Reinforced with Deverra tortuosa Vegetable Fibers
by
Tahani Zorgui, Hibal Ahmad, Mehrez Romdhane and Denis Rodrigue
J. Compos. Sci. 2024, 8(10), 394; https://doi.org/10.3390/jcs8100394 - 1 Oct 2024
Abstract
In this work, natural fibers extracted from the medicinal aromatic plant Deverra tortuosa, with different sizes (S1 = 2 mm and S2 = 500 μm), were incorporated into recycled low density polyethylene (rLDPE) to produce sustainable biocomposites. Compounding was performed with different
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In this work, natural fibers extracted from the medicinal aromatic plant Deverra tortuosa, with different sizes (S1 = 2 mm and S2 = 500 μm), were incorporated into recycled low density polyethylene (rLDPE) to produce sustainable biocomposites. Compounding was performed with different fiber concentrations (0 to 30% wt.) via twin-screw extrusion followed by injection molding. Based on the samples obtained, a comprehensive series of characterization was conducted, encompassing morphological and mechanical (flexural, tensile, hardness, and impact) properties. Additionally, thermal properties were assessed via differential scanning calorimetry (DSC), while Fourier transform infrared spectroscopy (FTIR) was used to elucidate potential chemical interactions and changes with processing. Across the range of conditions investigated, substantial improvements were observed in the rLDPE properties, in particular for the tensile modulus (23% for S1 and 104% for S2), flexural modulus (47% for S1 and 61% for S2), and flexural strength (31% for S1 and 65% for S2). Nevertheless, the tensile strength decreased (15% for S1 and 46% for S2) due to poor fiber–matrix interfacial adhesion. These preliminary results can be used for further development in sustainable packaging materials.
Full article
(This article belongs to the Special Issue Polymer Composites and Fibers, 3rd Edition)
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Open AccessArticle
Water Resistance Analysis of New Lightweight Gypsum-Based Composites Incorporating Municipal Solid Waste
by
Alicia Zaragoza-Benzal, Daniel Ferrández, Alberto Morón Barrios and Carlos Morón
J. Compos. Sci. 2024, 8(10), 393; https://doi.org/10.3390/jcs8100393 - 1 Oct 2024
Abstract
Incorporating waste to produce new environmentally friendly construction products has become one of the great challenges of the industry nowadays. The aim of this research is to analyse the behaviour of novel gypsum composites against water action, incorporating recycled rubber aggregates (up to
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Incorporating waste to produce new environmentally friendly construction products has become one of the great challenges of the industry nowadays. The aim of this research is to analyse the behaviour of novel gypsum composites against water action, incorporating recycled rubber aggregates (up to 8.5% vol.) and dissolved expanded polystyrene (up to 10.0% vol.). To this end, a total of 10 dosages have been proposed with the progressive substitution of natural resources by these secondary raw materials. The results show how it is possible to reduce the total water absorption of the gypsum composites by up to 8.3% compared to traditional gypsum material. In addition, it is also possible to reduce water absorption by capillary by up to 52.7%, resulting in lighter composites with good performance against water action. In all composites analysed, the mechanical strengths exceeded the minimum values of 1 MPa in bending and 2 MPa in compression, making them an optimal solution for the development of lightweight prefabricated products for damp rooms.
Full article
(This article belongs to the Special Issue Lightweight Composites Materials: Sustainability and Applications, Volume II)
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Thermomechanical and Viscoelastic Characterization of Continuous GF/PETG Tape for Extreme Environment Applications
by
José Luis Colón Quintana, Scott Tomlinson and Roberto A. Lopez-Anido
J. Compos. Sci. 2024, 8(10), 392; https://doi.org/10.3390/jcs8100392 - 30 Sep 2024
Abstract
The thermomechanical and viscoelastic properties of a glass fiber polyethylene terephthalate glycol (GF/PETG) continuous unidirectional (UD) tape were investigated using differential scanning calorimetry (DSC), thermomechanical analysis (TMA), and dynamic mechanical analysis (DMA). This study identified five operational conditions based on the Army Regulation
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The thermomechanical and viscoelastic properties of a glass fiber polyethylene terephthalate glycol (GF/PETG) continuous unidirectional (UD) tape were investigated using differential scanning calorimetry (DSC), thermomechanical analysis (TMA), and dynamic mechanical analysis (DMA). This study identified five operational conditions based on the Army Regulation 70-38 Standard. The DSC results revealed a glass transition temperature of 78.0 ± 0.3 °C, guiding the selection of temperatures for TMA and DMA tests. TMA provided the coefficient of thermal expansion in three principal directions, consistent with known values for PETG and GF materials. DMA tests, including strain sweep, temperature ramp, frequency sweep, creep, and stress relaxation, defined the material’s linear viscoelastic region and temperature-dependent properties. The frequency sweep indicated an increased modulus with rising frequency, identifying several natural frequency modes. Creep and stress relaxation tests showed time-dependent behavior, with strain increasing under higher loads and stress decreasing over time for all tested input values. Viscoelastic models fitted to the data yielded R2 values of 0.99, demonstrating good agreement. The study successfully measured thermomechanical and viscoelastic properties across various conditions, providing insights into how temperature influences the material’s mechanical response under extreme conditions.
Full article
(This article belongs to the Section Fiber Composites)
Open AccessArticle
Development and Improvement of a “Paper Actuator” Based on Carbon Nanotube Composite Paper with Unique Structures
by
Ryodai Toyomasu and Takahide Oya
J. Compos. Sci. 2024, 8(10), 391; https://doi.org/10.3390/jcs8100391 - 30 Sep 2024
Abstract
We propose a new type of soft actuator based on carbon nanotube (CNT) composite paper (CNTCP), i.e., a paper actuator. In our previous study, we demonstrated that actuator operation was possible when using CNTCPs as electrodes with ordinary paper containing ionic liquid between
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We propose a new type of soft actuator based on carbon nanotube (CNT) composite paper (CNTCP), i.e., a paper actuator. In our previous study, we demonstrated that actuator operation was possible when using CNTCPs as electrodes with ordinary paper containing ionic liquid between the electrodes; however, their bending motion was not sufficient. Therefore, we here attempt to modify the paper actuator. For this, we tried to soften CNTCPs by first reducing the ratio of contained CNTs. In addition, as a new strategy, we took advantage of the fact that the proposed actuator was made of paper and introduced the Kirigami (introducing periodical slits to papers) technique into the structure of our paper actuator. As a result, the performance of the actuator was improved, and its bending motion became visibly larger. The response of the improved actuator to the input voltage was investigated in detail, and the detailed operating conditions could be clarified. Moreover, it was found that not only a bending motion but also a twisting motion could be realized in specific slit patterns. It is thought that the fact that the variation in movement can be increased simply by adding incisions is unique to the proposed paper actuator.
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(This article belongs to the Special Issue Feature Papers in Journal of Composites Science in 2024)
Open AccessArticle
Tensile Properties and Weibull Modulus of Polymeric-Fiber-Reinforced Epoxy-Impregnated Bundle Composites
by
Kimiyoshi Naito, Chiemi Nagai and Shota Kawasaki
J. Compos. Sci. 2024, 8(10), 390; https://doi.org/10.3390/jcs8100390 - 30 Sep 2024
Abstract
The tensile properties and the Weibull statistical distributions of the tensile strength of poly-(para-phenylene-2,6-benzobisoxazole) (PBO), poly-(para-phenylene terephthalamide) (PPTA), copoly-(para-phenylene-3,4′-oxydiphenylene terephthalamide (PPODTA), polyarylate (PAR), and polyethylene (PE) polymeric fiber epoxy-impregnated bundle composites have been investigated. The results show that the Weibull modulus decreases as
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The tensile properties and the Weibull statistical distributions of the tensile strength of poly-(para-phenylene-2,6-benzobisoxazole) (PBO), poly-(para-phenylene terephthalamide) (PPTA), copoly-(para-phenylene-3,4′-oxydiphenylene terephthalamide (PPODTA), polyarylate (PAR), and polyethylene (PE) polymeric fiber epoxy-impregnated bundle composites have been investigated. The results show that the Weibull modulus decreases as the tensile modulus, strength, and inverse of the failure strain increase. The interfacial shear properties were also examined using the microdroplet composite. For the lower interfacial shear strength of polymeric fibers, the Weibull modulus decreases as interfacial shear strength increases. Conversely, for the higher interfacial shear strength of polymeric fibers, the Weibull modulus increases as interfacial shear strength increases. Interestingly, these inflection points were also observed for the 20–30 MPa interfacial shear strength.
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(This article belongs to the Section Polymer Composites)
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Open AccessArticle
The Impact of 3D Printing Technology on the Improvement of External Wall Thermal Efficiency—An Experimental Study
by
Beata Anwajler and Piotr Szulc
J. Compos. Sci. 2024, 8(10), 389; https://doi.org/10.3390/jcs8100389 - 30 Sep 2024
Abstract
Three-dimensional printing technology continues to evolve, enabling new applications in manufacturing. Extensive research in the field of biomimetics underscores the significant impact of the internal geometry of building envelopes on their thermal performance. Although 3D printing holds great promise for improving thermal efficiency
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Three-dimensional printing technology continues to evolve, enabling new applications in manufacturing. Extensive research in the field of biomimetics underscores the significant impact of the internal geometry of building envelopes on their thermal performance. Although 3D printing holds great promise for improving thermal efficiency in construction, its full potential has yet to be realized, and the thermal performance of printed building components remains unexplored. The aim of this paper is to experimentally examine the thermal insulation characteristics of prototype cellular materials created using 3D additive manufacturing technologies (SLS and DLP). This study concentrates on exploring advanced thermal insulation solutions that could enhance the energy efficiency of buildings, cooling systems, appliances, or equipment. To this end, virtual models of sandwich composites with an open-cell foam core modeled after a Kelvin cell were created. They were characterized by a constant porosity of 0.95 and a pore diameter of the inner core of the composites of 6 mm. The independent variables included the different material from which the composites were made, the non-uniform number of layers in the composite (one, two, three, and five layers) and the total thickness of the composite (20, 40, 60, 80, and 100 mm). The impact of three independent parameters defining the prototype composite on its thermal insulation properties was assessed, including the heat flux (q) and the heat transfer coefficient (U). According to the experimental tests, a five-layer composite with a thickness of 100 mm made of soybean oil-based resin obtained the lowest coefficient with a value of U = 0.147 W/m2·K.
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(This article belongs to the Special Issue Sustainable Composite Construction Materials, Volume II)
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